Filtration
Separating insoluble solids from liquids using filter paper.
Practise Analytical, Lab & Spectroscopy All Analytical, Lab & Spectroscopy topics
Separating insoluble solids from liquids using filter paper.
Practise Analytical, Lab & Spectroscopy All Analytical, Lab & Spectroscopy topics
Filtration separates an insoluble solid from a liquid by passing the mixture through a porous medium such as filter paper, which retains the solid as the residue while the liquid passes through as the filtrate. Gravity filtration is simple and suits most precipitates, while vacuum filtration through a Buchner funnel is faster and gives drier solids. Folded filter paper increases surface area and speeds up gravity filtration. The collected solid is usually washed with a small portion of cold solvent to remove adhering solution, which carries dissolved impurities. The particle size of the precipitate determines the choice of filter, since very fine particles can pass through or clog the paper.
Key ideas: For a precipitate to be analysed, use quantitative filter paper that burns to negligible ash or a sintered glass crucible. Decant most of the liquid first, wash the precipitate with small portions of cold solvent, and test the filtrate for completeness of precipitation. Use a short stem funnel for fast gravity filtration. Dry to constant mass for gravimetry.
Common mistakes and connections: Common errors are using too much wash liquid (which dissolves product), filling filter paper above its rim, and tearing the paper under suction. Students also confuse residue with filtrate. Hot filtration to remove insoluble impurities must be done with preheated apparatus to prevent crystals forming in the funnel. Related to gravimetric analysis and crystallization.
Filter media retain different particle sizes; fine precipitates such as calcium carbonate need a finer paper or membrane to avoid passing into the filtrate. The interactive lesson shows this as a live animation or chart.
Collecting a calcium carbonate precipitate formed when sodium carbonate is added to calcium chloride solution.
Separating insoluble solids from liquids using filter paper.
Filtration is a beginner topic in Analytical, Lab & Spectroscopy. It needs no earlier chemistry lessons and is a good starting point.
Study these earlier topics in Analytical, Lab & Spectroscopy first: Standard Solutions, Primary Standards, Volumetric Glassware.
The next topics in Analytical, Lab & Spectroscopy are Distillation and Fractional Distillation.
Yes. The interactive lesson includes a self-check question on Filtration, and the Analytical, Lab & Spectroscopy quiz draws on every topic in this area.
Filtration is topic 21 of 99 in Analytical, Lab & Spectroscopy.